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Tube and Tube Fittings, Nickel-Chromium-Molybdenum Alloy

Scope
Description
Tube lengths and tube fittings fabricated from tube lengths, Nickel-ChromiumMolybdenum
Alloy, in the following inch OD (outside diameter)
sizes: 1/4, 3/8, 1/2, 3/4, and 1
Material Specification UNS N06022

Inch OD                     ASTM Specification
1/4, 3/8                        B 622
1/2 to 1                          B 622, B 626

Dimensional
Specification
Inch OD                   Wall Thickness (Inch)
1/4, 3/8                            0.035
1/2                                     0.049
3/4 to 1                              0.065
Purchase
Order
Purchase order (PO) shall specify the following:
1. Surface roughness [default: ≤ 0.6 µm (25 microinch) Ra]
2. Seamless or welded [default: seamless]
3. Certificate of Conformance requirements (See the Certification Section of this
specification.)
Lengths Tube lengths shall be 6 m (20 ft) nominal, 5.5 m (18.5 ft), minimum.
Fitting linear dimensions shall be per supplier-provided drawings.
Tolerances

Acceptance Criteria

Inch OD              [ OD                  Ovality ]                      Quantity to be Inspected
1/4, 3/8                  ± 0.004               ± 0.004                                             10%
1/2 to 1                   ± 0.005                ± 0.005                                              10%

Face Squareness

1/4 to 3/4                                        ± 0.5°                                                       10%
1                                                   ± 0.010 inch                                                 10%

Wall Thickness

All sizes                        ± 10% of nominal wall thickness                            10%

Fitting Dimensions

All sizes                              ± 0.8 mm (1/32 inch) linear,                             10%
± 0.5° angular tolerance from
dimensions on supplier drawings

Drawings Supplier shall provide drawings that specify all dimensions of tube fittings.
Calculations Not required
Chemical Composition Per UNS N06022
Mechanical Strength Per ASTM B 622 and ASTM B 626
Welding Longitudinal seam butt welded tube to be manufactured as EFW without added filler metal. Following are seamless and welded size requirements:
Inch OD                        Seamless/Welded
1/4, 3/8                               seamless
1/2 to 1                         seamless (welded optional)
Inspection Visual Inspection: All components shall be 100% visually inspected under bright
white light to verify that the internal surfaces show no sign of surface imperfections
(e.g., tool marks, draw marks, scratches, pits, graininess, orange peel, hazing, weld
discoloration, spots, stains, residues) or visible particulate contamination.

Dimensional Inspection: Components shall be dimensionally inspected for
conformance to the acceptance criteria specified in the Tolerances Section of this
specification.

Testing Parameter                               Acceptance Criteria                                     Quantity Tested/Test Method

Surface Finish Testing:

Surface roughness                   ≤ 0.6 µm (25 microinch) Ra                                  0.5%/SEMASPEC
or value specified in the PO                                         90120400B-STD
Helium (He) Leak Testing:
Inboard Leak Rate                          ≤ 1 x 10-9 sccs                                                         100% of fittings

with circumferential welds/
-6
Outboard Leak Rate                           ≤ 5 x 10-6  sccs                                         SEMASPEC 90120391B-STD

Particle Count Testing:

Particles ≥ 0.20 micron                           0                                                                  1  part per lot/
Particles ≥ 0.10 micron                      ≤ 0.036 ptc/L (1 ptc/ft3)                          SEMASPEC 90120390B-STD
Particles ≥ 0.02 micron                       ≤ 0.36 ptc/L (10 ptc/ft3)

Gaseous Impurity Testing:

Parameter                                                               Acceptance Criteria                Quantity Tested/Test Method
Moisture                                                             ≤ 0.5 ppm (molar)                           1 part per lot/SEMASPEC 90120397B-STD
Oxygen                                                               ≤ 0.5 ppm (molar)                             1 part per lot/SEMASPEC 90120398B-STD
Total Hydrocarbons                                         ≤ 0.5 ppm (molar)                            1 part per lot/SEMASPEC  90120396B-STD

Examination None
Certification Certified Test Report per ASTM A 450/A 450M (EN 10204, Type 3.1 in Europe)
from the alloy-producing mill shall be submitted for each mill heat utilized.

Certificate of Conformance: A Certificate of Conformance shall be submitted with
each shipment of purchased components. The certificate shall include supplier
verification that components conform to specification requirements.

For all orders, certificate shall include verification of the following:
• Helium leak testing performed on 100% of welded components
• Visual Inspection performed on 100% of components
• Dimensional inspection performed on 10% of components
• Cleaning performed on 100% of components, also note Cleaning Specification
revision number and date

• Single-bag packaging performed on 100% of components
• Note the Air Products purchase order number, supplier lot number, mill heats
utilized to fill order, shipping order number, date, and signature of supplier’s
Quality Control Representative
When specified in the PO, certificate shall include verification of the following:
• Surface finish testing performed
• Particle count testing performed
• Gaseous impurity testing performed

Marking All tube lengths and tube fittings shall be marked as follows:
• Manufacturer’s name or unique symbol
• “Seamless” or “welded”
• Serial number or lot number
• Heat number within 24 inches of each end
• Part number (tube fittings only)
Protection None
Color Coding Not required
Packing Packaging: Packaging shall be performed in a Class 100 cleanroom or clean zone.
Each component shall be purged prior to capping using 99.999% pure, 0.01 micron
filtered nitrogen. Both component end connections shall be sealed by pressing
polyethylene caps over 45 micron (1.75 x 10
-3
inch) thick polyamide squares. Then
each component shall be bagged in 150 micron (6 x 10
-3
inch) thick polyethylene
sleeves or bags. Bag shall be vacuum sealed or purged. When purge sealing, purge
gas shall be entrapped inside bag prior to sealing.

Shipment Packing: Components shall be packed for shipment so that damage will
not occur to the bagging or components. All shipments of 25 kilograms (50 pounds)
or greater shall be packaged inside wooden crates or plastic cases. Components
shall be packed in the crate/case using shock-absorbing spacers and keepers. Voids
shall be filled with shock-absorbing materials. Additionally, wooden crates shall be
inner lined with polyethylene sheet and outer wrapped with stretch plastic. The
supplier shall guarantee quality and cleanliness upon delivery to Air Products. Any
component that is received by Air Products in a damaged condition shall be returned
and replaced, all at the supplier’s expense. Damage also includes a torn bag and
loss of purge gas environment.

Special
Requirements
Cleaning: Cleaning shall be performed in a Class 100 cleanroom or clean zone.
Cleaning of tube and fittings shall be performed per supplier’s cleaning specification.
A final rinse shall be made with deionized water and the effluent shall be monitored
for resistivity. The acceptable resistivity level is ≥ 17.5 megaohm-cm. The following is
a recommended cleaning method:

Step 1: Wash by submerging in multi-stage continuous counterflowing deionized
water baths. Final rinse with a 60°C (140°F) deionized water spray.

Step 2: Dry by purging with 99.999% pure, 0.01 micron filtered, 60°C (140°F)
nitrogen. For fittings, bake off residual moisture by using a vacuum oven or a heat
lamp.

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