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Face Seal Fittings, TP316L EP Technical Specification | SEMI F20

This article is about Face Seal Fittings, TP316L EP Technical Specification and technical specification based on international codes and standards of SEMI F20.

Face Seal Fittings, TP316L EP Technical Specification | SEMI F20

Scope
Description
Face seal fittings, TP316L stainless steel with EP (electropolished) inner surface, in the following tube sizes: 1/8, 1/4, 3/8, 1/2, 3/4, 1 inch OD (outside diameter).
Gaskets, unplated or silver-plated TP316L stainless steel, or unplated or silver-plated nickel. Gasket retainer assemblies shall be made available for sizes 1/4 to 1 inch OD.
Material
Specification
Fittings shall be Grade TP316L stainless steel per SEMI F20.
Dimensional
Specification

Inch OD                          Wall Thickness (Inch)
1/8                                         0.0281/4, 3/8                                0.035
1/2                                         0.049
3/4, 1                                     0.065

Purchase
Order
Purchase order (PO) shall specify the following:
1. Tube size
2. Gasket material [default: unplated nickel]
3. Gasket retainer type [default: no gasket retainer]
4. Surface roughness [default: ≤ 0.25 µm (10 microinch) Ra]
5. Melt process [default: AOD]
6. Manganese content [default: ≤ 2.00 %]
7. Certificate of Conformance requirements (See the Certification Section of this spec.)
Lengths Fitting dimensions shall conform to supplier-provided cut sheets and drawings.
Tolerances

Face Seal Fittings, TP316L EP Technical Specification | SEMI F20

Acceptance Criteria

Inch OD                    OD          Ovality                                   Quantity to be Inspected
1/8                           ± 0.003  ± 0.003                                                    10%
1/4,3/8                   ± 0.004  ± 0.004                                                     10%
1/2 to 1                   ± 0.005   ± 0.005                                                     10%

Face Squareness

1/8 to 3/4                   ± 0.5°                                                                    10%
1                                   ± 0.010 inch                                                         10%

Wall Thickness

All sizes                       ± 10% of nominal wall thickness                     10%

Fitting Dimensions

All sizes                         ± 0.8 mm (1/32 inch) linear,                              10%
± 0.5° angular tolerance from
dimensions on supplier drawings

Drawings Supplier shall provide drawings that specify all dimensions of fittings.
Calculations Not required
Mechanical
Strength
ASTM A 632 Grade TP316L (UNS S31603), DIN 17457/DIN 17458
Welding Orbital butt welded fittings shall be manufactured as EFW without added filler metal.
Heat
Treatment
Hardness shall be per ASTM A 269 for Grade TP316L (UNS S31603).
Inspection Visual Inspection: All components shall be 100% visually inspected under bright white
light to verify that the internal surfaces show no sign of surface imperfections (e.g., tool
marks, draw marks, scratches, pits, graininess, orange peel, hazing, weld discoloration,
spots, stains, residues) or visible particulate contamination.
Dimensional Inspection: Components shall be dimensionally inspected for conformance
to the acceptance criteria specified in the Tolerances Section of this specification.
Testing

Face Seal Fittings, TP316L EP Technical Specification | SEMI F20

Surface Finish Testing:

Parameter                             Acceptance Criteria                                   Quantity Tested/Test Method
Surface roughness              ≤ 0.25 µm (10 microinch) Ra                 0.5%/SEMASPEC 90120400B-STD
or value specified in the PO
Chromium to iron ratio       ≥ 1.5:1                                                        0.5%/SEMASPEC 90120403B-STD
Oxide thickness                     ≥ 20 angstroms

Surface defect count             ≤ 40 at 3500X ± 100X                            0.5%/SEMASPEC 90120401B-STD

Helium (He) Leak Testing:

Inboard Leak Rate                          ≤ 1 x 10-9 sccs                                 100% of fittings with circumferential welds/
Outboard Leak Rate                       ≤ 5 x 10-6 sccs                                 SEMASPEC 90120391B-STD

Particle Count Testing:

Particles ≥ 0.20 micron                               0                                              1 part per lot/
Particles ≥ 0.10 micron ≤ 0.036 ptc/L (1 ptc/ft3)                                SEMASPEC 90120390B-STD
Particles ≥ 0.02 micron ≤ 0.36 ptc/L (10 ptc/ft3)

Gaseous Impurity Testing:

Parameter                                   Acceptance Criteria                                   Quantity Tested/Test Method
Moisture                                     ≤ 0.5 ppm (molar)                               1 part per lot/SEMASPEC 90120397B-STD
Oxygen                                        ≤ 0.5 ppm (molar)                               1 part per lot/SEMASPEC 90120398B-STD
Total Hydrocarbons                 ≤ 0.5 ppm (molar)                                1 part per lot/SEMASPEC 90120396B-STD

Examination None
Certification Certified Test Report per ASTM A 450/A 450M (EN 10204, Type 3.1B in Europe) from the
steel-producing mill shall be submitted for each mill heat utilized.
Certificate of Conformance: A Certificate of Conformance shall be submitted with each
shipment of purchased components. The certificate shall include supplier verification that
components conform to specification requirements.
For all orders, certificate shall include verification of the following:
• Helium leak testing performed on 100% of welded components
• Visual Inspection performed on 100% of components
• Dimensional inspection performed on 10% of components
• Cleaning performed on 100% of components; also note Cleaning Specification
revision number and date
• Double-bag packaging performed on 100% of components
• Note Air Products purchase order number, supplier lot number, mill heats utilized to
fill order, shipping order number, date, and signature of supplier’s Quality Control
Representative
When specified in the PO, certificate shall include verification of the following:
• Surface finish testing performed
• Particle count testing performed
• Gaseous impurity testing performed
Marking All fittings shall be marked as follows:
• Manufacturer’s name or unique symbol
• “TP316L”
• Serial number or lot number
• Heat number
• Part number
Protection None
Color Coding Not required
Packing Packaging: Packaging shall be performed in a Class 100 cleanroom or clean zone.
Each component shall be purged prior to capping using 99.999% pure, 0.01 micron filtered
nitrogen. Both ends shall be sealed by pressing polyethylene caps over 45 micron
(1.75 x 10-3 inch) thick polyamide squares. Then each component shall be double bagged
in 150 micron (6 x 10-3inch) thick polyethylene sleeves or bags. Each bag shall be
independently vacuum sealed or purged. When purge sealing, purge gas shall be
entrapped inside each bag prior to sealing.Shipment Packing: Components shall be packed for shipment so that damage will not
occur to the double bagging or components. All shipments of 25 kilograms (50 pounds) or
greater shall be packaged inside wooden crates or plastic cases. Components shall be
packed in the crate/case using shock-absorbing spacers and keepers. Voids shall be filled
with shock-absorbing materials. The supplier shall guarantee quality and cleanliness upon
delivery to Air Products. Any component that is received by Air Products in a damaged
condition shall be returned and replaced, all at the supplier’s expense. Damage also
includes a torn bag and loss of purge gas environment.
Special
Requirements
Electropolishing: After heat treatment (and any subsequent welding, bending, or forming), all inner surfaces shall be electropolished to the acceptance criteria defined in the Testing Section of this specification.

Final surface passivation: After electropolishing, surfaces shall be passivated. Suggested passivation method is soaking in nitric acid (20% to 50% concentration) for ≥ 30 minutes.

Cleaning: After final surface passivation, cleaning shall be performed in a Class 100 cleanroom or clean zone. Cleaning of tube and fittings shall be performed per supplier’s Cleaning Specification. A final rinse shall be made with deionized water, and the effluent shall be monitored for resistivity. The acceptable resistivity level is ≥ 17.5 megaohm-cm.
The following is a suggested cleaning method:

Step 1: Wash by submerging in multi-stage continuous counter-flowing deionized water baths. Final rinse with a 60°C (140°F) deionized water spray.

Step 2: Dry by purging with 99.999% pure, 0.01 micron filtered, 60°C (140°F) nitrogen. For fittings, bake off residual moisture by using a vacuum oven or a heat lamp.

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